ARCOS Inductively Coupled Plasma Emission SpectrometerMain technical features:
Spectro Analytical Instruments, a German company, is a large professional manufacturer of emission spectrometers. It has its own application technology center and spare parts bonded warehouse in Shanghai, responsible for developing instrument analysis methods according to user needs, guiding users to better utilize all functions of the instrument, and providing application training for users, so that they have no worries.
1. High optical resolution: The optical resolution of 165-340nm remains constant at 0.0085nm, and above 340nm it remains constant at 0.015nm. Whether for resolution testing, sensitivity testing, or actual sample analysis, the resolution remains constant at the above values.
2. Specially designed ultraviolet optical system: using a closed argon filled optical system combining Paschen Runge one-dimensional spectroscopy and multi CCD, it enables analysis of spectral lines below 190nm without the need for time-consuming and gas intensive chamber blowing, and can be analyzed immediately upon startup. Such as analyzing P (sensitive lines 177nm and 178nm), S (180nm and 182nm), Al (sensitive line 165nm), Pb (168nm), etc.
3. Maintenance free generator: A maintenance free generator designed with air cooling, which does not require a cooling circulating water system and is truly maintenance free.
4. Strong sample adaptability: Using a high-power solid-state generator with a frequency of 27.12MHz and a power range of 700-1700W, adjustable every 1W, the sample adaptability is *, and it can directly inject and analyze samples such as oil products and high salt solutions that require * instrument load requirements.
5. Detector without refrigeration: Due to the use of first-order spectral lines for analysis, the sensitivity is high, so there is no need to force the refrigeration detector to reduce noise to improve analysis sensitivity, and there is also no need to waste argon gas blowing the detector. Power on and start the ignition test, truly "ready to use"
6. Non overflow detector: All instruments adopt a linear detector array of about 29 blocks, each detector has an independent data processing unit, and independent analysis parameters (including integration time, etc.) can be set separately for each spectral line, without the common "overflow phenomenon" of two-dimensional detectors. Due to the independent data processing system of the detectors, the analysis time is extremely fast, and the full spectrum of the sample can be collected in 3 seconds. And it can be used in conjunction with other instruments such as HPLC (high-performance liquid chromatography), with a measurement frequency of 10 times per second.
7. Precise airflow control: The plasma gas (with a control accuracy of 0.1L/min), auxiliary gas, and atomization gas (with a control accuracy of 0.01L/min) are all controlled by mass flow computers, which can greatly ensure the stability of the instrument's test results. Generally, other manufacturers only use mass flow control for atomization gas in ICP.
8. Fully automatic control of observation height: All adopt computer-controlled precise observation height (vertical observation type) or flame and OPI interface distance (horizontal observation type). In addition, all torch tubes adopt a quick installation design, which can quickly locate the height of the torch tube and its concentricity with the coil.
9. Wide dynamic linear range: The dynamic linear range is 108.
10. True post analysis capability: During each analysis, the instrument can automatically save all spectral lines of all elements in all samples, including the standard sample. After the analysis is completed and the instrument is turned off, new elements or spectral lines can be directly added to the spectrum, and the background position or correction method of the working curve can be changed without the need for re injection analysis.
11. Complete spectral line library: In addition to providing a complete NIST standard spectral line library, it also provides recommended spectral line library, optimal spectral line library, interference spectral line library and other convenient methods for users to establish or analyze spectra. In addition, users can directly add spectral lines.
12. Observation interface: OPI ™ (Level)/SPI ™ (Vertical): OPPETRO ICP's Cold Cone Interface (OPI) ™), Significantly improve analysis sensitivity and testing accuracy while eliminating tail flame interference, without the need for auxiliary vertical observation. SPI ™ The interface ensures that all optical paths are isolated from air interference during vertical observation, improving the sensitivity of ultraviolet spectral lines.
13. Convenient and practical automatic peak identification: It can automatically qualitatively identify any peak in the sample, bringing great convenience to the analysis of unknown samples.
ARCOS Inductively Coupled Plasma Emission SpectrometerSpectral system:
Maintain a constant temperature of+15 degrees Celsius+-0.1 degrees Celsius
Paschen Longroland Circle Design
750mm focal length
Holographic concave original grating, with a line density of 2 × 3600 lines/mm and 1 × 1800 lines/mm
Grating material
Magnesium fluoride optical components
All are level 1 wavelength coverage
• Wavelength range 165-770nm
• Incident slit 15 microns
Detector:
29 linear CCDs carefully selected and optimized based on their wavelength are arranged continuously on a Roland circle
Each CCD has 3648 pixels
Pixel resolution: 165-340nm 3pm,>340nm 6pm
The optical system maintains a constant temperature of+15 degrees Celsius+-0.1 degrees Celsius
Parallel readout design
Each CCD has its own signal processing system
Intelligent data acquisition and data elimination system
The dynamic range is 108
• Short integration time of 1 millisecond
A short measurement time of 2 seconds (including full spectrum detection and assignment)
The integration time is automatically optimized based on the signal strength of each pixel
• Full wavelength coverage
• Automatic dark current correction
• Automatic wavelength position standardization
TCP/IP communication interface
UV optical system
UV optical system
The light chamber is filled with argon gas and sealed without consuming blowing gas
Dual incidence window, easy to maintain
• Automatic argon purification system
RF generator
• Self exciting type
The frequency is 27.12MHz
• Output power: 0.7-1.7KW
• Energy efficiency: 70%
Power stability<0.1%
• Plasma automatic ignition
Low power, low argon gas flow standby mode
• All computer-controlled
Air cooling (no additional cooling equipment required)
Solid state power generator
OPI interface
The OPI interface of Spectro is very powerful. This technology uses horizontal observation to improve sensitivity by an order of magnitude while greatly reducing matrix interference in traditional horizontal observation.
• Purge the external light path with argon gas
• Argon flow rate 0.5-0.8 L/min
Can directly analyze samples with a solid content of up to 20%
Plasma position
Fully computerized automatic control and optimization of the position between plasma and observation cone
The plasma position, generator power, and various gas flow rate parameters are controlled by a computer and stored in the analysis method. As long as the method is called up, all parameters are automatically adjusted to their desired positions.
The preset analysis conditions can be adjusted very reliably without the need for further optimization operations. Since the plasma position can also be automatically adjusted during the analysis process, it can be adjusted according to the needs of each element if necessary
Horizontal adjustment: adjustment accuracy of 0.1mm
Sample injection system and torch tube components
• Easy to disassemble injection system bracket
• Hot injection chamber
• Fully computer-controlled airflow velocity
Plasma gas: adjustment accuracy of 0.1 l/min
Auxiliary gas: adjustment accuracy of 0.01 l/min
Atomizing gas: adjust accuracy to 0.01 l/min
O * Additional gas: adjustment accuracy of 0.01 l/min
• Additional oxygenation control system
The standard sample injection system consists of the following components:
O Integrated torch tube
Cross type atomizer
O (dual channel) atomization chamber
Note: There are many other injection systems available for selection (see attached system).
Computer controlled 70 speed, 4-channel, 12 roller peristaltic pump for sample injection
• Quick pre rinsing and quick cleaning function
Peristaltic pump discharges waste liquid
*Option: Data processing system (computer system, low configuration, upgrade at any time)
In dual core, 2.9GHz
2048 memory
320GB hard drive
DVD burning drive
CD burning software
• Graphics adapter
• 2 PCI slots
• Keyboard
• Mouse
USB interface
• Serial port
• Parallel port
• Sound card
• 2 network adapters
• XP ™ operating system
• LED display
• Inkjet printer
Basic functions:
Professional version of Windows XP operating system
• User interface
Carefully arranged clear and intuitive operations
• Stacked toolbar, automatic or user-defined interface
Task oriented menu structure
Multi tasking system
• Powerful multi-level user and access authorization management
Users can set various alarm reminder systems
-Users can define their reactions to information, events, error warnings, and other related messages
-If necessary, automatically transmit various data through transmission
-Instrument Usage Report Checklist
Advanced ODBC/ADO databases
Advanced data integration and security systems
User and Data Management System for CFR11
HTML based help system including technology
Analysis Window
• Equipped with various analysis and display functions
-Simultaneous display of various samples
-Scalable multiple repeated analysis/or average result display
-It can simultaneously display analysis results, spectra and standard curves, and display the working status of instruments such as RF generators and automatic samplers
Each sample can input various definition words
• Customized dilution engineering calculation
Users can define the molecular formula and directly display the molecular content
• Blank correction
• Matrix correction
• Automatic interference correction
• Simultaneous background correction
Flexible selection of various reference elements and spectral lines for simultaneous internal standardization
• Automatic standardization
Optimization of automatic atomizer
• Automatic control of sample testing
-Output result
-Comparison of preset control indicators
-Marking of excessive results
• Compliant with EPA/GLP standards
• Instantaneous signal measurement mode
• Signal acquisition rate 10Hz
Reserved interfaces with peripheral devices
• Can display the analysis results of each spectral line element in various concentration units
The analysis results can be displayed in concentration or intensity
• Can display statistical data (such as the average and relative sum of each measurement result with respect to standard deviation)
Sample labeling, each test result, mean, standard deviation, raw data (parameters can be pre-set for each analysis method):
-Various analysis report templates (including user-defined templates)
-Various data reporting modes can be used (PDF/HTML/RTF)
-Printer
-Data storage
The analysis results and raw data can be output to ASCII mode
• Can be cut or pasted onto a clipboard
According to the standard curve definition range, it is possible to automatically select spectral lines and switch between spectral lines
Record samples and standard analysis results in full spectrum or specific frequency bands
Output spectra (individual and average spectra) to ASCII
All analysis results can be reprocessed across the entire spectrum
• Data reprocessing
• Full spectrum storage for each analysis
All analysis spectral line parameters can be edited and corrected after the analysis process is completed
Add new elements or spectral lines to the measured sample
The analysis results are revised based on peak height or peak area, and the background is reset
Reset or revise internal standards
Add new or revised calibration curve models
Re evaluate the completed work curve or standardization
• Retrospective analysis of previous sample results
Method editing function
• Task guide guidance method editing process
• Powerful and editable spectral line library (NIST)
• Automatically select specific suggested spectral lines
• Standard unit library
Standard sample spectral line library: Different concentration units can be used for each element during sample analysis
Conduct semi quantitative analysis
If necessary, specific excitation parameters and torch positions can be selected for specific spectral lines
Specific spectral lines can be defined using peak height or peak area
According to the standard curve definition range, it is possible to automatically select spectral lines and switch between spectral lines
User defined molecular weight calculation (e.g. composite elements, element price range)
Various models can be used for automatic interference correction
• Automatic interference correction
Simultaneous online and/or offline background correction
- Primary or secondary models
-Background extrapolation
Interactive Background Selection Preview
- No need to define measurement range
• Method input and output
Can be calculated using standard curves of one, two, or three powers
Can calibrate any number of samples
• Standard added features
Correction of numerical and graphical outputs between all elements
Simultaneously display a list of calibration samples and coefficients for each analyzed spectral line
Various sample weight models
• File server functionality
• Define automatic backup analysis methods and analysis results
• Intelligent recovery function
Spectral display function
• Record or display stored spectra function
• Rapid semi quantitative analysis
• Automatic spectral line recognition
• Complete spectral line library (NIST)
• Jiapu Line Library
• Recommended spectral line library
• Identification of interference spectral lines
• Spectral line scaling function
Automatic observation
• Easy to use sample list, powerful scripting language
Task oriented structure - several methods can be included in one list
Using scripting languages similar to BASIC can program complex automated tasks
Scripts can include logical variables, basic mathematical operations, and functions defined by users using variables (integers, floating-point numbers, logical variables, strings)
• List of easy-to-use samples for standard automated tasks
The automatic sample list and script mode support the following functions:
Automatically control plasma startup through time or events
Generator automatic standby function
Automatic flushing and shutdown of the generator
Method of flushing
Intelligent mobility and flushing
Definition and Control of Screen Display Automatic Sample Injector
Each batch/time can have no * samples
Supports complete cutting/pasting and pasting to the clipboard
Automatic standardization of time or event control, sample determination, blank correction, calibration, calibration addition to calibration, conditional dilution
Programmable automatic event operation, such as automatic standardization if the control sample exceeds the standard
Sample repeat determination function
Dynamic measurement correction
? Bracket
When the sample exceeds the curve range, it will automatically dilute
Sample priority function
Process control that complies with US EPA regulations
random file
Operation Manual
External component description
size
Spectrometer size: 1074 x 1610 x 753 mm (height X width X depth)
Foot size: 1367 x 692 mm (length x width)
weight
• Weight: Approximately 250kg
environmental conditions
• Room temperature: 18-35? C
Ideal working temperature of 18-25? C( 64-77?)
Relative humidity:<80%, no condensation
• Non corrosive gases and dust
Exhaust requirements
Ability: 2 x 250 cubic meters per hour less, with independent control of wind speed for two exhaust ducts
Requirements for argon gas
Purity: 99.996%
• Pressure: 7.5 bar (109 psi)
• Consumption: 10-18 l/min
Power requirements
•230 VAC ± 5%, 50/60 Hz
• Power consumption: approximately 4.5 kilowatts
30-32A online fuse
